This document is a lecture/laboratory manual dealing with the analysis of selected organic pollutants. It is intended for use by those having little or no experience in the field, but having one year (or equivalent) of college organic chemistry, and having basic laboratory skills (volumetric glassware, titration, analytical and trip balances). Topics include: dissolved oxygen, biochemical oxygen demand, ammonia, nitrates, nitrites, carbon analysis, chemical oxygen demand, surfactants, oil and grease phenolics, gas chromatography, and polychlorinated biphenyls. (BB)