Highly efficient microwave-assisted organic synthesis is now commonplace in both industry and academia. Recently, a conductively heated sealed-vessel reactor was introduced that acts very similarly to a microwave reactor and is more affordable. Application of such reactors in teaching laboratories is advantageous because of the restricted window…

The current literature on test equating generally defines it as the process necessary to obtain score comparability between different test forms. The definition is in contrast with Lord's foundational paper which viewed equating as the process required to obtain comparability of measurement scale between forms. The distinction between the notions…

Contribution: The scheme for virtual emulation experiments based on discrete logic which appropriately lowers students' cognitive burden and possesses manipulatable interactive logic in tune with real experiments is put forward. The relationship between students' experiential learning and the influence of cognitive burden is also discussed.…

The formation of chemical patterns is in general difficult to control due to the random diffusive motions of the reacting chemical species in solution. In this paper, we present a new method using audible sound to control the formation of chemical patterns obtained in blue bottle experiments. The waves generated on the surface of the solution by…

Electrochemistry represents a powerful sustainable method for chemical synthesis; however, its widespread application is limited due to the lack of exposure and appropriate basic training of synthetic chemists and engineers in electrochemistry and electrochemical engineering. The introduction of diverse laboratory practices to the current…

The purpose of this publication is to present a novel approach to the demonstration of the Dzhanibekov effect. The main idea of our version is to use a lightweight spinning top of a spherical external form but distinct principal moments of inertia floating in the upward flow of air. As a result, the Dzhanibekov effect can be easily demonstrated…

We investigated a very long chain falling from the pile on the edge of a table to the floor both experimentally and theoretically. In this very simple and novel configuration we showed that the velocity of the chain quickly converges to its asymptotic value, and that the steady-state velocity is proportional to the square root of the height of the…

The measurement of the charge-to-mass ratio, e/m, of the electron is a fundamental part of any study of electricity and magnetism. It is possible to use an apparatus designed to measure e/m for other things, including investigations of electron flow through a near vacuum, measuring a work function, and even exploring some quantum mechanics…

Our first experience of dimension typically comes in the intuitive Euclidean sense: a line is one dimensional, a plane is two dimensional, and a volume is three dimensional. However, following the work of Mandelbrot, systems with a fractional dimension, "fractals," now play an important role in science. The novelty of encountering…

Tumescence in cadaveric dissection involves the introduction of fluid into interstitial spaces to assist in the separation of natural tissue planes and the preservation of delicate structures. With a hand surgeon's perspective, the senior author brought this technique into the cadaver lab. The infusion helped transform desiccated and adherent…

Diffraction refers to a kind of optical phenomena which occurs when light approaches an element (object or aperture) whose features are in the range of the illuminating wavelength (small apertures, sharp edges). It can be explained by means of the undulatory nature of light or also geometrically by using simple ray optics. Diffraction phenomena…

In this paper, a simple method is described for visually demonstrating that the wavelength of light reduces when entering a medium of higher refractive index. When a violet laser (405 nm) is reflected off the surface of a Blu-ray disc (track spacing 320 nm) diffraction cannot occur since the wavelength is greater than the track spacing. However,…

Students determine the iron mass in dietary supplements using four colorimetric assays. These colorimetric assays were selective for Fe[superscript 3+]. It was complexed by thiocyanide, salicylate, gallic acid, and Fe(CN)[subscript 6][superscript 4-], forming blood-red, red, violet, and blue complexes, respectively. The [lambda][subscript max] of…

Applying the idea of green chemistry, we extended an esterification teaching experiment with isoamyl alcohol and acetic acid and reused isoamyl acetate in the transesterification reaction with KOH as the catalyst. As a result, isoamyl alcohol was produced and could be reused for the teaching experiment. The simplified experimental method achieved…

Benzoin, an [alpha]-hydroxy ketone, is stereoselectively reduced by sodium borohydride to yield hydrobenzoin, the stereochemistry of which is determined by acetalization and analysis of the derivative by NMR spectroscopy. This classical experiment has been enhanced by modern spectroscopic and computational analysis to enable students to…