An experiment for the undergraduate organic chemistry laboratory involving a method for the isolation of eugenol from cloves has been developed. The experiment employs microwave-assisted extraction (MAE) of the essential oil from whole cloves using aqueous ethanol and the subsequent isolation of eugenol by acid-base extraction. The MAE allows for…

This work presents an outline for a full-quartile design-based learning laboratory-based course suitable for final year Bachelor's students. The course has been run for 5 years in the department of Chemical Engineering and Chemistry. The course attempts to provide a complete laboratory experience for its students, including an authentic research…

A computational laboratory experiment investigating molecular models for hexagonal boron-carbon-nitrogen sheets (h-BCN) was developed and employed in an upper-level undergraduate chemistry course. Students used the Avogadro user interface for molecular editing and the WebMO interface for the quantum computational workflow. Density functional…

Synthesis and characterization of nanomaterials yields opportunities for instruction of related topics in solution chemistry and materials science, as well as spectroscopy connecting to band theory, the "particle in a box" quantum mechanical model, and thermodynamics. In collaboration with an undergraduate research assistant, we have…

Student-built photometers are recognized as being useful tools in teaching laboratories that help students understand the concepts behind experimental measurements, and several devices have been reported that employ photoresistors as the detector of choice. We demonstrate here an improvement over these instruments and the analyses thereof,…

Apparatus catalogues of the first half of the 20th century contain a number of clever and simple devices for measuring the index of refraction of a liquid. In some cases students can put together one of these pieces of apparatus and then make their own measurements. The Gilley board was one of the devices that caught my eye, and I would like to…

Single-case experimental designs (SCEDs) are a useful tool for evaluating the effects of interventions at an individual level and can play an important role in the development and validation of evidence-based practices. Historically, researchers relied on visual analysis of SCED data and eschewed statistical approaches. Although researchers…

Potassium tris(oxalato)ferrate(III) trihydrate is a commonly prepared coordination compound in general or upper-level chemistry laboratories and can be recycled to grow large single crystals that instructors may display when introducing the experiment to classes. Showing the crystal's shape can also be used to briefly introduce students to X-ray…

Substitution reactions of alcohols are some of the simplest experiments performed in undergraduate organic chemistry laboratory settings. However, the use of gas chromatography (GC) as an analytical tool for these reactions can be at times laborious and time-consuming. In this work, 1-pentanol, 2-pentanol, 3-pentanol, and 2-methyl-2-butanol were…

This work presents two electronic systems experiments with resonance tubes, which generate automatically a sequence of several sound wave frequencies in a range defined by the user and then verifies the amplitude of each one in real-time, allowing for the immediate data visualization in a graph. Besides, they save all the frequency values and the…

Polymer chemistry is essential within chemical education because of its applications in academic and industrial research, materials science, and across engineering disciplines. Teaching polymer chemistry principles early on in the undergraduate curriculum allows students to find connections between chemistry and real-world applications and can…

Real-time quantitative PCR is a technique used to monitor the PCR reaction in real time. RT-qPCR is broadly classified into two types based on its purpose: absolute and relative quantification. Absolute quantification is used in a wide array of fields such as microbiology, food technology, and biotechnology to quantify the microbiological…

An easy circuit for measuring the power of a solar panel in physics classroom by using the microcontroller Arduino will be introduced in this article. The measured data is transferred via Bluetooth to the smartphone app 'phyphox' where it is displayed graphically. The circuitry enables measuring the power of a solar panel in different situations…

Optimization of experimental conditions in chromatography is recognized as a wear-and-tear process involving hundreds of experiments in order to maximize the number of separated compounds for each sample. The critical thinking skills and practices entailed cannot be achieved with students in a conventional lecture class. This report provides a…

The use of smartphones in experimental physics is by now widely accepted and documented. PASCO scientific's Smart Cart, in combination with student-owned smartphones and free apps, has opened a new universe of low-cost experiments that have traditionally required cumbersome and expensive equipment. In this paper, we demonstrate the simplicity,…