Thermogravimetry coupled with Fourier transform infrared spectroscopy (TG-FTIR) is a useful technique for the thermal and structural characterization of materials at academic and research levels. This paper describes an experiment for chemistry students to understand the use of TG-FTIR for advanced qualitative and quantitative thermal analysis…

Contribution: This article presents a teaching experiment platform for an undergraduate laboratory program designed to fulfill the needs of control engineering classroom experiment teaching. The teaching experiment platform is a cost-effective teaching tool that can be promoted on a large scale in colleges and universities. The teaching experiment…

The falling rod paradox, i.e. the fact that the tip of an almost horizontal rod falls with an acceleration 'higher than g', when the other end is hinged or supported, is a popular physics demonstration. It can be visualized by placing e.g. a coin on the tip of the rod and fixing a cup next to the coin. When the rod is released the free-falling…

This Article comes from a series of 2 h instrumental analysis laboratory experiments developed in response to social distancing requirements established because of the coronavirus pandemic (COVID). The experiments provided rich data-analysis opportunities that taught students the chemical principles that underpin instrumental techniques, yet made…

Novel biomaterial development is a rapidly growing field that is crucial because biomaterial fouling, due to rapid and irreversible protein adsorption, leads to cellular responses and potentially detrimental consequences such as surface thrombosis, biofilm formation, or inflammation. Therefore, biomaterial technology's fundamentals, like material…

A laboratory experiment that exposes students to fundamental concepts in kinetics and statistical thermodynamics to study systems of great current interest in nanotechnology by employing a foundational technique in physical chemistry is described. A modified commercial flash photolysis spectrometer was used to study photoinduced isomerization…

As ongoing digitalization accelerates the execution of experiments and the documentation and storage of the corresponding data substantially, appropriate research data management (RDM) is a necessity to enable sustainable research at all. Consequently, a rethinking is currently taking place in academia. This process becomes visible by the…

We discuss the use of a simple piece of equipment made of a 50 mL syringe attached to a 2 mL graduated pipet to demonstrate Boyle's law and Charles's law. A plot of the hydrostatic pressure against the reciprocal of the volume of the gas read from the equipment is linear as discussed in the paper and gives the atmospheric pressure at the…

This two-period undergraduate laboratory experiment involves the synthesis of a mixture of isomeric unknowns, isolation of the mixture by means of distillation, and characterization of the two products primarily by NMR spectroscopy (1D and 2D) supported with IR spectroscopy and GC-MS techniques. Subsequent calculation and examination of the…

This lab experiment uses [superscript 31]P NMR spectroscopy of biomolecules to determine pK[subscript a] values and the binding energies of metal/biomolecule complexes. Solutions of adenosine nucleotides are prepared, and a series of [superscript 31]P NMR spectra are collected as a function of pH and in the absence and presence of magnesium or…

In hydrostatics, pressure measurement with U-gauges and their relationship to density is a well-known experiment. Very little is studied or experimented with the dynamics of the movement of a liquid in a U-tube probably due to its theoretical complexity but, after all, it is a simple damped oscillating system. In this paper we present a relatively…

This laboratory experiment utilizes an exploration of the storage stability of beer to introduce basic aspects of electron-paramagnetic-resonance (EPR) spectroscopy. Radicals formed upon aerobic forced-aging of beer samples are established by using a spin-trap. The students are introduced to basic principles of EPR spectroscopy and food and…

This two-part laboratory experiment is concerned with investigating key aspects of the Suzuki-- Miyaura cross-coupling reaction. The first part of this experiment utilizes high-throughput experimentation techniques to reinforce, explore, and extend fundamental concepts that are presented in the classroom. In contrast, the second part employs…

For a variety of reasons, understanding oxidation-reduction (redox) reactions can be challenging for introductory chemistry students. To provide an experiential foundation for students to learn redox concepts, we developed a laboratory experiment that frames redox reactions as a simulated murder mystery. In this experiment, permanganate, which…

A practical experiment is described to estimate the distance to a star using simple equipment, suitable for secondary or undergraduate students. The brightness of the star is visually matched to a miniature filament lamp, and its distance inferred from the inverse square law. Students gain an appreciation of astronomical units and practice in…