Elemental analysis is performed in a variety of ways in food and environmental sciences; thus, we have designed an activity in which students gain experience with research-level lab techniques in a real-world context through the quantification of key elements in breakfast cereals using microwave plasma optical emission spectroscopy (MP-OES). The…

Raman scattering is a powerful tool for revealing the vibrations of molecules, but as a nonlinear optical phenomenon, its signals can change via mechanisms like resonance enhancement that have no direct analogue in infrared spectroscopy. In this work, complementary measurements conducted on 4-nitrophenol and its conjugate base allow students to…

As electrochemistry continues to gain broader acceptance and use within the organic chemistry community, it is important that advanced undergraduate students are exposed to fundamental and practical knowledge of electrochemical applications for chemical synthesis. Herein, we describe the development of an undergraduate laboratory experience that…

As the need for online or virtual science courses grows, it is important to incorporate laboratory work into these courses. However, it is difficult to find cost-effective ways to integrate the laboratory work, especially as campuses across the world have had to quickly transition to the online learning environment in the midst of the COVID-19…

We present an experiment designed to hone the decision-making skills of (undergraduate) chemistry students by using aqueous crossed aldol reactions. Here, we present two simple crossed aldol reactions based on inexpensive and readily available materials: The condensation of vanillin and cinnamaldehyde with acetone. The procedure uses the variation…

Biodiesel is an important alternative fuel synthesized by the trans-esterification of vegetable oils, animal fats, and recycled greases. In this experiment, students prepared biodiesel through the base-catalyzed trans-esterification of several vegetable oils, which were subsequently analyzed in comparison with conventional petroleum-based fuels to…

The implementation of an integrated approach to upper-level undergraduate chemistry laboratory instruction that incorporates student choice both in the selection and sequencing of the experimental work is presented. The approach involves combining laboratory work in several traditional subdisciplinary areas of chemistry in a single course.…

In order to introduce the concept of covalent organic frameworks (COFs), an important class of predictable crystalline porous polymers, an integrated laboratory experiment for advanced organic chemistry students is reported. The importance of these kind of polymers and their multiple applications are presented as a part of key concepts in polymer…

Synthesis and characterization of nanomaterials yields opportunities for instruction of related topics in solution chemistry and materials science, as well as spectroscopy connecting to band theory, the "particle in a box" quantum mechanical model, and thermodynamics. In collaboration with an undergraduate research assistant, we have…

Student-built photometers are recognized as being useful tools in teaching laboratories that help students understand the concepts behind experimental measurements, and several devices have been reported that employ photoresistors as the detector of choice. We demonstrate here an improvement over these instruments and the analyses thereof,…

Structure--activity relationships are foundational concepts in biochemistry and drug design. Despite their importance, it can be difficult to create and execute laboratory activities that allow students to directly observe the interactions between small-molecule drugs and their biomolecular targets. Here, we report an activity that investigates…

This article describes a ten week long laboratory exercise designed for undergraduate students aimed at enhancing their understanding of physiological and biochemical responses of plants under dehydration stress. Hypothesis was built around previous reports which suggested that exogenous application of certain elicitors leads to transient…

University of Michigan--Dearborn offers a one semester, two credit, stand-alone Organic Chemistry Laboratory course aimed at students with an interest in health-related careers. The COVID-19 pandemic led to a campus closure and a subsequent transition to a partially remote laboratory curriculum developed on-the-fly for the Winter 2020 semester…

A remote experiment was developed and carried out to create a phenol/water phase diagram using a low-cost automated data collection system and an online video broadcast. Both the data and video from the experiment were transmitted in real-time. The remote lab experiment was evaluated using qualitative and quantitative questionnaires filled out by…

Teaching emulsion polymerization is an important benchmark in undergraduate polymer courses. However, the introduction of hands-on experiments in undergraduate polymer laboratories is challenging: experimental time, reagents, and equipment involved are the primary restraints. We report a practical emulsion polymerization laboratory experiment for…