Metal-organic frameworks (MOFs) are a class of porous materials that are often crystalline with high surface area and structural tunability. In this laboratory experiment designed for inorganic chemistry students at the undergraduate level, students complete a two-step experiment where they will first (i) synthesize two isostructural…

Calculating analytical uncertainties as a part of method validation is a relevant aspect of field and laboratory practices in instrumental analytical chemistry subjects, which usually require complex algorithms. This work describes the development and didactic use of an automatic and straightforward informatics tool, implemented in an Excel macro,…

Titration is an important experimental skill that every chemistry educator and learner must master. Titration is often the method of choice in the science laboratory courses in secondary and postsecondary schools. During acid-base titration, chemistry learners are always told about salt formation. However, a practical visualization of the salt…

The demand for sustainable synthetic methods in modern industry has been increasing rapidly due to the requirements of environmental protection and energy conservation, which has brought organic electrochemical synthesis to the forefront nowadays. Here, a two-part laboratory experiment has been designed to train undergraduates in comprehending and…

Scientists have always been fascinated by transient far-from-equilibrium systems. Since the (early) 1970s, there have been literature reports on the implementation of didactic experiments as a tool for attracting and stimulating students' and general public interest. In this work, a group of 12 high school students, supported by their chemistry…

A Maker-oriented experimental course in general chemistry has been created by using digital tools, such as a computer, a pressure sensor, and data processing software, in combination with a new multiple expansion method and laboratory equipment to determine the vapor pressure precisely. In this Maker chemistry experiment, the pressure sensor…

The preparation of ethyl acetoacetate is a distinctive, century-old classic organic chemistry laboratory project. Ethyl acetate and sodium metal (sodium ethoxide) are reacted by Claisen ester condensation to produce the sodium salt of ethyl acetoacetate and then obtain the refined product by acidification as well as washing, drying, and…

A chemistry laboratory experiment is described to introduce undergraduate college students to membrane separation technology. This experiment combines a simple nanowire membrane fabrication and visually indicated molecule separation. The membrane is produced via coprecipitation synthesis followed by a filtration assembly process, which can be…

The process of method development is at the heart of analytical chemistry, yet direct experimental experience with the process is rarely taught in the undergraduate laboratory. We report here an experiment that uses rapid, safe, and inexpensive paper-based microfluidics with cell phone detection in order to facilitate the development of a…

If a ball rolls in a circular path on a horizontal surface at constant speed then its horizontal rotation axis changes direction with time. A simple experiment is presented showing that the torque applied to the ball is equal to the rate of change of its angular momentum, even though the magnitudes of its angular velocity and angular momentum…

Here we demonstrate how data from the clinical pulmonary function lab can help students learn about the principle of airway-parenchymal interdependence. We examined the relationship between airway conductance (Gaw) and lung volume (thoracic gas volume, TGV) in 48 patients: 17 healthy; 20 with emphysema, expected to have reduced airway-parenchymal…

The knowledge of the mechanical properties of polymers and other materials is essential for several tasks in the field of materials science, like component design and material development. The tensile test is one method of determining many of the material's most defining mechanical characteristics. However, the teaching of laboratory experiments…

In this study, it is aimed to develop practical teaching activities that can be used in optics teaching. For this purpose, a virtual laboratory environment was created in RayLab which is an application for design and simulation of optics on the iPad/iPhone. In this context, the dispersion of white light in the prism, the relationship between the…

We investigated physics students' behavior in a second-year laboratory by analyzing transcribed audio recordings of laboratory sessions. One student group was given both a problem and procedure and asked to analyze and explain their results. Another was provided with only the problem and asked to design and execute the experiment, interpret the…

Introductory lab courses have been a staple of the physics curriculum for over 100 years. Yet these courses are now poised for change as recent research shows that they do not meet a frequent goal of enhancing student understanding of lecture content. In thinking about how to move forward, a look back at experiment courses in history seems wise.…