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NMR Spectroscopy in an Advanced Inorganic Lab: Structural Analysis of Diamagnetic and Paramagnetic Ni(II) Schiff Base Complexes
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Venable, T. Leon – Journal of Chemical Education, 2019
In a two-step synthesis starting with Ni(CH[subscript 3]COO)[subscript 2] ยท4H[subscript 2]O and salicylaldehyde, students prepare Nethyl and N-isopropyl Ni(II) Schiff base (imine) complexes. After isolation and recrystallization, the products are characterized by room-temperature magnetic susceptibility measurements, FTIR spectroscopy, and…
Descriptors: Spectroscopy, Inorganic Chemistry, Science Laboratories, Advanced Courses