Capstone teaching laboratory activities can serve as a crucial part of the undergraduate learning experience. With this in mind, a laboratory activity that combines synthesis and multiple characterization techniques has been developed for an upper-division, laboratory-based inorganic course. Complexes of Cu(II) and Ni(II) of the amino acid glycine…

This three-part laboratory experiment investigates key aspects of the Buchwald-Hartwig amination cross-coupling reaction through guided-inquiry learning strategies. The first part of this experiment utilizes high-throughput experimentation techniques to reinforce, explore, and extend fundamental concepts that are represented in the classroom,…

Italian high school students carried out some activities within career guidance actions organized by the Department of Chemistry of Sapienza University (Rome) in order to promote enrollments in a chemistry Bachelor's course, thus remedying the shortage of professional chemists. Novel didactic sequences have been designed to facilitate the…

Instrumentation plays a vital role in almost every area of chemistry. As such, it is imperative that the undergraduate curriculum is designed to allow students to have opportunities to use a variety of instruments to best prepare them for careers in chemistry. Previous work has provided evidence of the types of instruments students use in…

Accuracy and precision are measures of experimental error and are fundamental to most chemical analysis laboratory classes. Assessment of accuracy and precision is often based on the comprehension of the results generated by students rather than on the quality of the data generated. This activity focused on developing a chemical analysis…

[This paper is part of the Focused Collection on Instructional labs: Improving traditions and new directions.] We present the pedagogical design and implementation of "ESSENCe": Experimental problem solving using Staging, Scaffolding, Embedded information sources, iNstruments, and Collaboration. Research in experimental physics requires…

A laboratory experiment is described in which students carry out immobilization of the enzyme invertase via entrapment in alginate (Ca-alginate) and, accordingly, estimate values for kinetic constants and mass transfer coefficients. Immobilization of enzymes, or confinement thereof to a defined space with retention of most catalytic activity, is…

The principles of chemical kinetics comprise one of the core topics that appear throughout chemistry. Standard kinetics lessons typically cover reaction rates and relative rates, rate laws, integrated rate laws, half-lives, collision theory, and the Arrhenius equation. They can also introduce a discussion of mechanisms as well, which may be the…

In this laboratory experiment, the synthesis and characterization of H[subscript 5]PV[subscript 2]Mo[subscript 10]O[subscript 40]@Cu[subscript 3](BTC)[subscript 2] (denoted as NENU[subscript -9], H[subscript 3]BTC = 1,3,5-benzenetricarboxylic acid) and its application in fuel desulfurization were performed. This experiment is designed for advanced…

This article describes a simple setup of electrospinning using widely available resources. The Arduino board, an electronic platform that is commonly accessible was adapted for a controller. Specifically, recycled parts consisting of plastic gears and a lipstick case were incorporated for the construction of a syringe pump. A cheap DC-DC converter…

Induced seismicity has received a lot of attention in recent years. This new natural phenomenon appeared as a result of active human influence on nature. The phenomenon has been detected in places of natural gas and oil recovery, and geological storage of CO[subscript 2]. One of the main reasons for the observed seismic activity is associated with…

Is the reductionist approach to teaching chemical principles in the laboratory adequate for students to make effective evaluations? In this work, using the example of sunscreens, students first assessed the analytical chemistry parameters of the active ingredients, later comparing and contrasting them with organic chemistry information for…

This paper provides seven topics on sodium hydrogen carbonate (NaHCO[subscript 3]) and its ions for readers looking for familiar material phenomena to strengthen students' understanding of the chemical concepts of thermodynamics. The first concept is the ideal gas law, followed by the van't Hoff equation, Gibbs energy, pH change, chemical…

Eleven different laboratory experiments were designed and executed throughout a semester to provide a meaningful research experience for 23 undergraduate biochemistry majors at UTSA. The topic of the semester was based on the idea of exploring new aspects to enhance our understanding of how the human body uses cytochrome P450 enzymes to metabolize…

The electrolysis of water to produce hydrogen is a critical step in many green chemistry processes. The key to the efficiency of water electrolysis is the synthesis of an appropriate electrocatalyst. Three-dimensional (3D) printing is an increasingly important part of many industrial processes. In this study, we propose an efficient laboratory…