At the University of South Australia (UniSA), Biochemistry is a second year undergraduate course. The student cohort is diverse, with students enrolled in courses with a laboratory focus, such as Laboratory Medicine, Medical Science, Nutrition and Food Science and Pharmaceutical Science. The course is taught in a traditional manner, with weekly…

This two-period undergraduate laboratory experiment involves the synthesis of a mixture of isomeric unknowns, isolation of the mixture by means of distillation, and characterization of the two products primarily by NMR spectroscopy (1D and 2D) supported with IR spectroscopy and GC-MS techniques. Subsequent calculation and examination of the…

This lab experiment uses [superscript 31]P NMR spectroscopy of biomolecules to determine pK[subscript a] values and the binding energies of metal/biomolecule complexes. Solutions of adenosine nucleotides are prepared, and a series of [superscript 31]P NMR spectra are collected as a function of pH and in the absence and presence of magnesium or…

In hydrostatics, pressure measurement with U-gauges and their relationship to density is a well-known experiment. Very little is studied or experimented with the dynamics of the movement of a liquid in a U-tube probably due to its theoretical complexity but, after all, it is a simple damped oscillating system. In this paper we present a relatively…

This laboratory experiment utilizes an exploration of the storage stability of beer to introduce basic aspects of electron-paramagnetic-resonance (EPR) spectroscopy. Radicals formed upon aerobic forced-aging of beer samples are established by using a spin-trap. The students are introduced to basic principles of EPR spectroscopy and food and…

This two-part laboratory experiment is concerned with investigating key aspects of the Suzuki-- Miyaura cross-coupling reaction. The first part of this experiment utilizes high-throughput experimentation techniques to reinforce, explore, and extend fundamental concepts that are presented in the classroom. In contrast, the second part employs…

For a variety of reasons, understanding oxidation-reduction (redox) reactions can be challenging for introductory chemistry students. To provide an experiential foundation for students to learn redox concepts, we developed a laboratory experiment that frames redox reactions as a simulated murder mystery. In this experiment, permanganate, which…

The study of vibration in uniform beams provides physics teachers with a platform by which a broad range of physics vibration-related topics can be explored without expensive and specialized equipment. This paper presents two laboratory exercises related to lateral beam vibrations. These exercises use beam theory coupled with free sound-analysis…

Since at least the 1960s, organic chemistry textbooks have featured pK[subscript a] tables for organic acids that include values for H[subscript 2]O and H[subscript 3]O[superscript +] (15.74 and -1.74, respectively) that are thermodynamically and chemically indefensible. Here we trace this error back to Brønsted's early contributions in the 1920s…

The nucleophilic aromatic substitution reaction and thia-Michael addition using thiourea as an odorless, cheap, and easy-to-handle sulfur source in water are described, which can be used to teach upper-division undergraduates the role of thiourea in the formation of C-S bonds and the principles of green chemistry. The use of a cheap, nontoxic…

The interface of art and science provides a broad range of educational and collaborative projects at various learning stages. Therefore, the use of historic artists' materials for teaching chemistry is receiving more attention. We prepared and used copper acetate (verdigris pigment) for a series of interconnected, lab-based activities, which can…

A concept for undergraduate mechanics courses at universities is introduced where traditional pencil-paper based exercises are partially replaced by experimental exercises, in which smartphones are used as measurement devices. A detailed guidance for practical realization and implementation of these tasks formats into the course is presented.…

Faculty in the Department of Chemistry and Physics at the University of New England (UNE) have recently transformed introductory and advanced chemistry curricula by embedding the high impact practice of undergraduate research. Course Based Undergraduate Research Experiences (CUREs) have provided experiential learning opportunities for over 272…

Bioinorganic topics are ubiquitous in the inorganic chemistry curriculum; however, experiments to enhance understanding of related topics are scarce. In this proposed laboratory, upper undergraduate students assess the biological interaction of molybdenocene dichloride (Cp2MoCl2) with bovine serum albumin (BSA) by fluorescence spectroscopy.…

Being able to contextualise and solve complex problems is a highly valued skill in STEM graduates--a skill which we strive to nurture in our students. Since its introduction into undergraduate teaching, laboratory teaching has been used to consolidate students conceptual understanding, develop their practical skills and inculcate an evidence based…