The substitution of carbonyl compounds with liquid bromine as a brominating agent is the most commonly employed synthesis method for a-bromoacetophenone and its derivatives. However, liquid bromine possesses certain drawbacks, such as volatilization, high toxicity, strong corrosion, and poor reaction selectivity, which limit its application and…

This paper uses the questionnaire to evaluate the current status of laboratory safety perceptions, willingness, and efforts of first-year undergraduates at the School of Chemistry and Chemical Engineering, Tianjin University of Technology. The survey includes a sample size of 360 undergraduates covering four chemistry-related majors. The…

The Joint Safety Team (JST) was conceived in 2012 by the Departments of Chemical Engineering and Materials Science and Chemistry at the University of Minnesota and the Dow Chemical Company as a model student-led safety organization. The JST initiative was aimed at improving academic safety through four core areas: compliance, awareness, resources,…

In this article, a proven safety concept with documented success is presented. The concept aligns with best safety practices and the international engineering educational framework termed "The CDIO Initiative," and it has resulted in a strong safety culture among students and staff. This concept has been developed for undergraduate…

Developing strong safety cultures in academic institutions requires that students at all levels be educated by faculty in chemical safety. Yet chemical safety education is missing from the chemistry curriculum. This article considers a report of numerous injuries from incidents from using flammable chemicals in demonstrations as evidence that…

A relatively large number of organic and inorganic chemistry reagents are air- or moisture-sensitive, and undergraduate students should be trained in their use. When handling such reagents, it is important to select the correct syringe and to use that syringe correctly. We have found that the best syringe for use in an undergraduate setting is a…

Chemometric techniques such as partial least-squares (PLS) regression have been applied with huge success to a wide array of chemical problems including multicomponent analysis of analytes in complex mixtures. Despite this, there are few examples of laboratory pedagogical exercises that involve students in the acquisition of chemical data from…

While lab accidents that involved personal injuries or significant property damage are required to be reported by law, many minor lab incidents or near misses are less frequently reported, especially in an academic research environment. However, public awareness of these stories and incidents create valuable learning opportunities and can prevent…

The chemistry of metal-organic frameworks (MOFs) has the potential to introduce high school and undergraduate students to the fundamental chemical principles of structure and bonding, enhance the development of skills in synthesis and crystal growth, and promote hands-on experience with gas capture and host-guest chemistry of emerging materials…

Laboratory work in chemistry has been extensively researched in the last decade but the gap between research and practice is still broad. This "Perspective" shares 10 guiding principles relating to university laboratory education, drawing on research over the last decade. Written with an audience of practitioners in mind, the…

A method to synthesize biaryls through the Suzuki-Miyaura cross-coupling reaction using a recyclable fluorous precatalyst is described. This laboratory experiment, which demonstrates the safety benefits of green chemistry, is integrated into an upper-division course. Besides simply using the catalyst for a reaction, students can reuse the catalyst…

"N"-Formamides are important intermediates in the synthesis of many pharmacologically active compounds and are used as protecting groups for amines or as catalysts in different reactions. The current "N"-formylation experiment is designed as a part of an introductory organic chemistry course for undergraduate students. The…

There currently exists a significant deficiency in the nuclear chemistry workforce within the United States, despite its importance in areas of medicine, national security, and energy. Poor coverage of this topic across many chemistry departments at the undergraduate level likely contributes to this shortage. Increasing interest and hands-on…

Smartphones, coupled with small mobile sensors, make it possible to work with near-infrared (NIR) spectroscopy in science classrooms. NIR spectroscopy has become a standard analytical technology in various industries. These new devices enable students to create their own data in real time. This article presents an inquiry-based teaching unit, in…

Techniques are needed to train students in "writing to learn", whose main goal is to "learn to write". This work aims to exemplify how writing can be a teaching learning technique in an example in Chemistry to develop a correct understanding of the preparation of molar solutions in the laboratory. It is essential that this is…