Laboratory chemical synthesis research typically lacks the preplanned hazard responses found in production-scale industrial laboratories. Chemical safety management is a known challenge in education-based facilities, which is concerning for academic and national laboratory environments working with inexperienced student researchers. At the…

The substitution of carbonyl compounds with liquid bromine as a brominating agent is the most commonly employed synthesis method for a-bromoacetophenone and its derivatives. However, liquid bromine possesses certain drawbacks, such as volatilization, high toxicity, strong corrosion, and poor reaction selectivity, which limit its application and…

A variety of strategies have been introduced to tackle the issue of laboratory safety in academic settings. These strategies include innovative educational tools as students transition from the classroom into the laboratory, the introduction of policies designed to protect the researchers in the laboratory environment, and the creation of teams of…

High-voltage plasma arcs from solid-state Tesla coils were used to produce characteristic atomic emissions of various metals. The colored arcs produced were highly visible and vibrant, making for a spectacularly engaging demonstration for groups of varying sizes. The demonstration used an inexpensive solid-state Tesla coil to generate low-current,…

This paper uses the questionnaire to evaluate the current status of laboratory safety perceptions, willingness, and efforts of first-year undergraduates at the School of Chemistry and Chemical Engineering, Tianjin University of Technology. The survey includes a sample size of 360 undergraduates covering four chemistry-related majors. The…

The Joint Safety Team (JST) was conceived in 2012 by the Departments of Chemical Engineering and Materials Science and Chemistry at the University of Minnesota and the Dow Chemical Company as a model student-led safety organization. The JST initiative was aimed at improving academic safety through four core areas: compliance, awareness, resources,…

The liquid nitrogen cloud demonstration is an effective, dramatic, large-scale demonstration to illustrate gas laws and cloud/fog (aerosol) formations for classes and large-scale outreach events. When performed at full scale, it is common to produce a cloud 20-30 feet in height. Its effect can be further enhanced by adding brightly colored…

In this article, a proven safety concept with documented success is presented. The concept aligns with best safety practices and the international engineering educational framework termed "The CDIO Initiative," and it has resulted in a strong safety culture among students and staff. This concept has been developed for undergraduate…

Insufficient knowledge of chemical hazards can cause unsafe behaviors, diseases, and accidents in the laboratory, hence educational interventions are significant. Due to its unique qualities, distance learning via educational applications has grown dramatically. This study aimed to determine the efficacy of a safety training intervention via…

In 2015, "NFPA 45, Standard on Fire Protection for Laboratories Using Chemicals," from the National Fire Protection Association (NFPA) was updated to include language requiring educators to perform a documented risk assessment when conducting demonstrations in K-12 classrooms. Additionally, in the past five years numerous organizations…

Developing strong safety cultures in academic institutions requires that students at all levels be educated by faculty in chemical safety. Yet chemical safety education is missing from the chemistry curriculum. This article considers a report of numerous injuries from incidents from using flammable chemicals in demonstrations as evidence that…

Chemical spillage has been measured for undergraduate students undertaking a laboratory practical designed to help develop their chemical handling skills. There was a low correlation found between the amount of chemical spilled and the ability to accurately carry out the primary goal of the experiment, which was to measure the concentrations of…

There is a scarcity of studies that focus on how South African high school physical sciences teachers are grappling with chemical laboratory safety (CLS). This is despite the fact that the Curriculum and Assessment Policy Statements in the South African school system increased emphasis on laboratory activities in the physical sciences. Department…

The Making Introductory Courses Real while Online (MICRO) laboratory project was developed to meet the need for hands-on experiments, focused on topics in analytical chemistry, to be delivered safely remotely or in a socially distanced in-person lab. Unlike more traditional lab experiments, MICRO laboratories use only microgram or nanogram amounts…

Chemometric techniques such as partial least-squares (PLS) regression have been applied with huge success to a wide array of chemical problems including multicomponent analysis of analytes in complex mixtures. Despite this, there are few examples of laboratory pedagogical exercises that involve students in the acquisition of chemical data from…