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Direct linkBain, Ryan M.; Pulliam, Christopher J.; Raab, Shannon A.; Cooks, R. Graham – Journal of Chemical Education, 2015
In this laboratory experiment, students learn how to use ESI to accelerate chemical synthesis and to couple it with on-line mass spectrometry for structural analysis. The Hantzsch synthesis of symmetric 1,4-dihydropyridines is a classic example of a one-pot reaction in which multiple intermediates can serve to indicate the progress of the reaction…
Descriptors: Chemistry, Laboratory Experiments, Science Experiments, Science Instruction
