Presents an improved technique for synthesizing acetanilide from nitrobenzene by reducing nitrobenzene with iron powder and hydrochloric acid. This experiment has been used successfully with 2,000 students during two semesters. (Author/SA)

Describes a laboratory experiment which demonstrates manipulation of highly reactive chemicals, use of a gas trap, and simple and reduced pressure distillation. Student must characterize starting material and product with nuclear magnetic resonance and infrared spectroscopy. (Author/SA)

Discusses the advantages of using small scale experimentation in the undergraduate organic chemistry laboratory. Describes small scale filtration techniques as an example of a semi-micro method applied to small quantities of material. (MLH)

Describes an organic chemistry experiment suitable for high school students in second year or an advanced chemistry course. The techniques for the extraction and purification of caffeine from various household materials are described. Further experimentation with the extracted caffeine is suggested. (LC)

An experiment is described which provides a simple example of the application of the Wittig reaction to the synthesis of unsaturated compounds. The experiment was designed with British HNC chemistry students in mind, but it is also suitable as a project-type exercise for final year GCE A-level students. (Author/BB)

Describes a procedure for freeing an element from either a mineral or organic matrix with the use of a radioactive tracer to determine recovery of the elements. (SLH)