Contained in this issue are 30 articles reviewing advances in different fields of analytical chemistry since 1980. Cumulatively, these reviews list over 1000 references. (CW)

Discussed is some of the confusion encountered in electrochemistry due to misunderstandings of sign conventions and simple mathematical errors. Clarified are issues involving emf series, IUPAC sign conventions, calculation of cell potentials, reference electrodes, the polarity of electrodes in electrochemical devices, and overpotential. (CW)

Explains some experiments involving thermal methods of analysis for undergraduate chemistry laboratories. Some experiments are: (1) the determination of the density and degree of crystallinity of a polymer; and (2) the determination of the specific heat of a nonvolatile compound. (HM)

Reviews background of atomic absorption spectrometry techniques. Discusses problems encountered and precautions to be taken in determining trace elements in the parts-per-billion concentration range and below. Concentrates on determining chromium in biological samples by graphite furnace atomic absorption. Considers other elements, matrices, and…

Describes an experiment combining qualitative and quantitative information from hydrogen nuclear magnetic resonance spectra. Reviews theory, discusses the experimental approach, and provides sample results. (JM)

Describes a comprehensive nuclear magnetic resonance (NMR) experiment designed to introduce undergraduate organic chemistry students to measurement/interpretation of NMR parameters. Students investigate chemical shift analysis, spin-spin coupling, peak integrations, effect of deuterium oxide extraction, and comparisons with literature spectra;…

Describes a low-cost instrument using a solar cell as a sensor to measure both instantaneous and integrated value of solar flux. Constructing and calibrating such an instrument constitutes an undergraduate experimental project, affording students an opportunity to examine a variety of aspects associated with solar energy measurements. (Author/SK)

Detailed is a method in which short pieces of teflon tubing may be used for collection tubes for collecting preparative fractions from gas chromatographs. Material preparation, laboratory procedures, and results of this method are discussed. (CW)

Using Fourier transformation methods in nuclear resonance has made possible increased sensitivity in chemical analysis. This article describes data acquisition, data processing, and the frequency spectrum as they relate to this technique. (CW)

Applications of lasers to molecular absorption spectrometry, molecular fluorescence spectrometry, visible semiconductor fluorometry, atomic absorption spectrometry, and atomic fluorescence spectrometry are discussed. Details of the use of the frequency-doubled diode laser are provided. (CW)

Describes three situations in which computer software was used in a chemistry laboratory. Discusses interfacing voltage output instruments with Apple II computers and using spreadsheet programs to simulate gas chromatography and analysis of kinetic data. Includes information concerning procedures, hardware, and software used in each situation. (CW)

Describes an experimental procedure to measure the specific heat of a gas. Discusses equipment, setup, and procedures and provides sample values obtained for air, propane, helium, carbon dioxide, and argon. (JM)

Describes an experiment on a coupled system in which accurate timing is carried out using a Light Activated Switch (LAS) technique. LAS can be used for a wide range of periodic phenomena, provided the amplitude is sufficiently large to interrupt a light beam. (Author/SK)

A description is given of an inexpensive nuclear magnetic resonance (NMR) spectrometer suitable for use in advanced laboratory courses. Applications to the nondestructive analysis of the oil content in corn seeds and in monitoring the crystallization of polymers are presented. (SK)