Presents a procedure used in sophomore level organic chemistry which has been particularly useful for organic qualitative analysis. Uses a nine-well spotplate and one-two mg of solid and three-four drops of eight different solvents. Solubility is checked at different temperatures. Provides a solubility table. (MVL)

Discusses a laboratory technique of enzyme purification by affinity chromatography as part of an undergraduate biochemical methodology course. Provides preparation details of the rat muscle homogenate and reagents. Proposes column requirements and assaying information. (MVL)

Describes a laboratory technique for quantitative analysis of caffeine by an isotopic dilution method for coupled gas chromatography-mass spectroscopy. Discusses caffeine analysis and experimental methodology. Lists sample caffeine concentrations found in common products. (MVL)

A 14-week, undergraduate-level Genetics and Population Biology course at Morgan State University was modified to include a demonstration of functional genomics in the research laboratory. Students performed a rudimentary sequence analysis of the "Caenorhabditis elegans" genome and further characterized three sequences that were predicted to encode…

Classroom discussion of scientific articles can be an effective means of teaching scientific principles and methodology to both undergraduate and graduate science students. The availability of classic papers from the American Physiological Society Legacy Project has made it possible to access articles dating back to the early portions of the 20th…

The problems involved when radiation-producing devices of our contemporary technology are used in the teaching of science at the high school and undergraduate college level are discussed. Information is provided on the hazards involved in the use of radiation-producing equipment or radioactive materials in science demonstrations and experiments…

A time-sharing FORTRAN program is described. It was created to allow a student to design and perform classical thermodynamic experiments on three models of a working substance. One goal was to develop a simulation which gave the student maximum freedom and responsibility in the design of the experiment and provided only the primary experimental…

Outlines an approach for instruction in a physical chemistry laboratory which combines traditional and project-like experiments. An outline of laboratory experiments and examples of project-like experiments are included. (BT)

Presents some introductory experiments involving the reaction between EDTA and several metal ions using metallochromic indicators. The experiments represent familiar reactions and are followed by suggestions for extension into areas of discovery work by students. (Author/SA)

Describes an experimental procedure to acquaint inorganic chemistry students with stereochemical concepts using tris-(2,3-butanediamine)cobalt(III). Notes two isomeric forms exist and both form metal chelates. Separation is accomplished by chromatography and analysis is by NMR and infrared spectroscopy. Provides spectra of isomers. (MVL)

Attempts to show that in the closed loops of cyclic structures the protons situated in conic regions above and below the ring will be shielded. Uses the diamagnetic and air stable octahedral tin(IV) complexes of porphyrins for study. Notes complexes crystallize easily and offer spectacular purple colors. (MVL)

This work describes outcomes of a research-driven advanced microbiology laboratory and literature research course intended to enhance undergraduate preparation for and contributions to original research. The laboratory section was designed to teach fundamental biochemistry and molecular biology techniques in the context of an original research…

Inquiry-based laboratories are acknowledged as the preferred method of instruction for development of research skills. Much has been written about changes in student performance associated with inquiry, but less is known about how students view the inquiry-based format or whether they perceive a benefit from this type of instruction. The Student…

Explains that triglycerides consist of a mixture of different compounds, depending on the total number of fatty acid constituents. Details the method and instrumentation necessary for students to analyze a vegetable oil for its triglyceride content. Describes sample results. (CW)

This experiment demonstrates the reduction of inorganic sulfate to sulfide in the pore water of estuarine muds. Procedures involve the incubation of mud samples for varying amounts of time followed by gravimetric determination. (Author/SA)