We report a series of experiments based upon cinnamon oil that were developed to provide a practical integration of green and sustainable chemistry concepts for the organic chemistry laboratory. Five experiments centering around cinnamaldehyde as a green, plant-based chemical were performed by undergraduate students in a second-year organic…

The ability to visualize chemical processes can be an asset in a teaching laboratory. Despite the advances in laboratory technology, apparatuses used in the teaching of simple thermodynamics concepts, such as exothermic/endothermic reactions, historically remain unchanged and can benefit from a fresh perspective. The recent incorporation of…

With the introduction of the Wireless Smart Cart by PASCO scientific in April 2016, we expect a paradigm shift in undergraduate physics laboratory instruction. We have evaluated the feasibility of using the smart cart by carrying out experiments that are usually performed using traditional PASCO equipment. The simplicity, convenience, and…

Technique-centered biochemistry or molecular biology undergraduate laboratory curricula do not offer significant opportunities for thoughtful, in-depth exploration of the science to foster investigative learning. To demonstrate inclusion of inquiry-driven laboratory experiments into the undergraduate biochemistry and molecular biology curricula, a…

Regioselectivity in hetero Diels-Alder reactions can be observed in a simple reaction between a nonsymmetrical heterodiene and an unsymmetrical heterodienophile. A 9 h and easy to implement laboratory experiment is described, in which students can observe the regioselectivity of inverse "electron-demand" hetero Diels-Alder reactions of…

Typical laboratory exercises for undergraduate organic chemistry students involve bulk phase reactions with work up of product. In this study, students performed accelerated versions of the Katritzky reaction of para-substituted anilines with pyrylium salts in three ways: (i) by dropcasting reagents onto a paper surface and allowing solvent to…

Teaching labs at the undergraduate level poses unique challenges to a school system forced online by COVID-19. We adapted physiology laboratories typically taught in-person to an online-only format, allowing students to measure personal health data alone. Students used available technology and low-cost devices for measuring respiratory and…

A Microsoft Excel workbook has been developed to simplify the quantitative analysis of experimentally measured titration curves for diprotic and triprotic amino acids such as glycine, arginine, histidine, and glutamate. Students perform the titration, enter the data into the worksheet, and manually adjust the resulting pK[subscript a] values to…

Einstein's relation between mass and energy is perhaps the most famous equation of Physics. Despite its simplicity, the meaning of E[subscript 0] = mc[superscript 2] is not easy to grasp. Furthermore, its traditional derivations rely either on the integral of "momentum," on properties of electromagnetic radiation, or even on the…

A modular experiment for upper-level undergraduate students is presented, featuring the product cycle and process evaluating the quality and quantity of biodiesel obtained from a microalgae feedstock grown under carbon-supplemented and nutrient-deprived conditions. Batch reactors are used to cultivate and harvest microalgae, which undergo…

The combination of organic synthesis and analytical chemistry into a related laboratory experiment is an excellent demonstration of the utility of making a compound to then be used further. Herein we describe an undergraduate laboratory experiment that involves the straightforward synthesis of an internal standard, ethyl 6-acetyloxyhexanoate, for…

We demonstrate that the simplicity of preparing functional microfluidic devices using 3D printing is well suited for undergraduate laboratories. Educational experiments utilizing non-paper-based microfluidic devices are often relegated to well-equipped, resource rich universities because traditional fabrication techniques require specialized and…

A safe, convenient, and environmentally benign laboratory experiment for the synthesis of biodiesel from six kinds of vegetable oils has been developed for the introductory organic chemistry laboratory. The experiment uses ultrasonic irradiation in the presence of a base catalyst at room temperature and atmospheric pressure. Because of safer and…

The implementation of an integrated approach to upper-level undergraduate chemistry laboratory instruction that incorporates student choice both in the selection and sequencing of the experimental work is presented. The approach involves combining laboratory work in several traditional subdisciplinary areas of chemistry in a single course.…

In order to introduce the concept of covalent organic frameworks (COFs), an important class of predictable crystalline porous polymers, an integrated laboratory experiment for advanced organic chemistry students is reported. The importance of these kind of polymers and their multiple applications are presented as a part of key concepts in polymer…