We adapted a classical asymmetric Michael addition for a 1 day experimental session (6-8 h) for third- or fourth-year undergraduate students. The experiment contains three steps: synthesis of a chiral Lewis acid, LiAl((S)-BINOL)[subscript 2], then its use as a catalyst in the Michael addition of diethyl malonate on cyclopentenone, followed by…

A fast, operationally simple, and reproducible synthetic protocol for anthraquinone dyes (AQDs), suitable for upper-division undergraduate industrial and organic chemistry laboratory courses, has been developed. This experiment is composed of three stages; the first step deals with the synthesis of AQDs, followed by a purification step, and…

A novel undergraduate analytical chemistry experiment involving the identification and quantification of linalool in essential oils was developed. The experiment uses the internal standard method with headspace solid phase microextraction (SPME) and gas chromatography--mass spectrometry (GC-MS). This method is applicable to any linalool-containing…

An integrated laboratory experiment was designed for introducing biochemistry students to basic static biochemistry to deepen their understanding on the properties and analysis of biomolecules such as total carbohydrates, lipid, protein, and protein-constituent amino acids. Food represents a very important source of biomolecules of technological…

In this study, we derived several formulas for the currents induced in a circular loop by a magnet connected to a spring-based simple harmonic oscillation system. In addition, we conducted an experiment for measuring the induced currents and compared the results with the theoretical prediction. It was confirmed that the prediction from the derived…

An introductory normal phase column chromatography experiment is described and evaluated for second year undergraduate chemistry laboratory class. The experiment involves a nucleophilic substitution yielding a crude mixture of reactant and one product, both of which are brightly colored and contrasting, creating a clearly visual separation when…

This project introduces green chemistry to the undergraduate laboratory through two pedagogical techniques: undergraduate research and guided-inquiry. Through these two learning activities, an efficient synthetic procedure for the PRINS cyclization of citronellal into isopulegol, focused on minimizing negative environmental impact, was developed.…

A drug discovery project has been successfully implemented in an advanced undergraduate organic chemistry laboratory. In the laboratory, a five-step synthetic sequence is used to prepare five analogues of 13-phenyl-1-tridecanol. These compounds are key precursors in the synthesis of 2-oxo-14-phenyltetradecanes. This class of compounds, isolated…

The use of radioactive isotopes in radioactive decay studies can be a problem due to the manipulation of radioisotopes, expensive equipment, and the difficulty of finding samples with a reasonable half-life (between 1 and 10 min). In this paper, we present a mock-up of a Geiger-Mu¨ller counter plus three fictitious radioisotopes. They form an…

Distance learning in physics is still facing challenges, mainly due to the difficult access to a laboratory for practical work. Practical work is an essential part of the physics classroom because it allows students to interact with authentic physics phenomena and develop their scientific abilities. In this paper, we propose alternative…

Polymer Chemistry is a subject in the Chemistry Programs, student have a natural curiosity about polymeric materials, that we use in our everyday activities. Our proposal is to apply cooperative learning in the Interfacial polymerization of Nylon 6,10 experimentation. The specific objectives of our project can be summarized as: To identify the…

The use of a multicompartment electrochemical cell for the potentiometric determination of solubility product constants of aqueous I[superscript -], Br[superscript -], SCN[superscript -], and Cl[superscript -] salts of silver is presented. An electrochemical cell presented in this study contained multiple half-cells made of disposable drinking…

The implementation of a laboratory exercise in an undergraduate chemistry course, where students perform a comparison of three different synthetic methods toward [Cu(Cl)(IPr)]-complexes (IPr = N,N'-bis(2,6-diisopropylphenyl)imidazol-2-ylidene), is described. The students are introduced to the continuous improvement of reactions in terms of green…

The essence of higher education is to cultivate innovative talents for the society. Hence, higher education institutions (HEIs), on the one hand, need to respond to social needs and government policies. On the other hand, they need to keep pace with the times and improve the details of teaching to improve the effectiveness of education. In this…

A laboratory experiment in which [superscript 1]H NMR and UV-vis spectroscopies are applied to probe the temperature dependence of a monomer-dimer equilibrium involving a cyclopentadienone derivative is described and discussed. Details of the data analysis for extraction of equilibrium constants from the raw experimental data from both techniques…