Presented is an activity in which the pH of a solution can be quantitatively measured using a spectrophotometer. The theory, experimental details, sample preparation and selection, instrumentation, and results are discussed. (CW)

Describes experiments in which students prepare in situ soluble complexes of metal ions with different ligands and observe and estimate the change in formal potential that the ion undergoes upon complexation. Discusses student formation and analysis of soluble complexes of two different metal ions with the same ligand. (CW)

Suggests a laboratory introduction to solid-solid phase transitions, thermochromism, and color changes associated with changes in ligand coordination suitable for undergraduate students in physical and general chemistry. Describes the preparation and analysis of the experiment. (CW)

Describes an apparatus that can be used to measure low gas pressures over a range of temperature in the undergraduate teaching laboratory. Discusses an experimental procedure and theory for pressure temperature measurements with this apparatus. (CW)

Described is a five-week introductory inorganic laboratory course for first-year undergraduate students. Included are details of three preparations and three analyses conducted by the students in the course. (CW)

Presents the construction aspects of a simple but reliable colorimeter made from locally available components. Notes the absorption range to be 400-750-nm. Lists seven experiments done on the instrument. (MVL)

Describes a physical organic experiment in thermodynamics and kinetics for undergraduate courses in organic chemistry, biochemistry, or physical chemistry. Details background information, solution preparations, equipment and methods, and the suggested experiments such as determination of general-base-catalytic coefficients and the Bronsted…

Describes a simplified redox method for total iron analysis suitable for execution in a three-hour laboratory period by general chemistry students. Discusses materials, procedures, analyses, and student performance. (CW)

Describes a laboratory experiment to determine the rate law for a substitution reaction of a transition metal. Derives the corresponding rate law from the accepted mechanism for the reaction using the steady state approximation and determines the conditions under which the two agree. (CW)

Described is an analytical method that may be used to replace the more difficult, traditional approach for the analysis of silicates. It is argued that this method allows the use of smaller samples and is more sensitive than other techniques. (CW)

Discussed are selected application and future trends in supercritical fluid chromatography (SFC). The greatest application for SFC involves those analytes that are difficult to separate using GC or LC methods. Optimum conditions for SFC are examined. Provided are several example chromatograms. (MVL)

Presents an experimental example illustrating the most common methods for the determination of kinetic parameters. Discusses the different theories and equations to be applied and the mechanism derived from the kinetic results. (CW)

Described is an inorganic chemistry course based on the premise that a balanced understanding of inorganic chemistry requires knowledge of the experimental, theoretical, and technological aspects of the subject. A detailed description of lectures and laboratories is included. (KR)

Describes a molar volume-molar mass experiment for use in general chemistry laboratories. Gives background technical information, procedures for the titration of aqueous hydrogen peroxide with standard potassium permanganate and catalytic decomposition of hydrogen peroxide to produce oxygen, and a discussion of the results obtained in three…

Describes a two-session experiment designed to provide a good illustration of, and to improve student knowledge of, the Grignard reaction and nucleophilic substitution. Discusses the procedure, experimental considerations, and conclusion of this experiment. (CW)