This guide is intended to support a high school specialization course in materials and processing technology. The document contains three sections: (1) information on using the material; (2) a set of instructor guides for eight instructional units; (3) 15 technological activity modules and teacher and student instructions for their use; and (4) resources. The set of instructor guides contains instructional units on an overview of materials and processing technology, technological procedures, materials technology fundamentals, construction technology fundamentals, manufacturing technology fundamentals, materials and processing technology, careers and leadership roles in materials and processing technology. Each guide contains a sample set of competencies, subject matter content, teacher plans and activities, student activities, and a list of resources and references. The technological activity modules are a set of representative activities that may be used to address each instructional unit's goals. The guide includes modules on problem solving, fiberglass fabrications, nondestructive testing, bridge construction, construction projects, concrete processing, jigs and fixtures, automated manufacturing, robotics, mass production, forming and managing a company, and career and leadership development. Each module includes an instructor component (objectives, competencies, materials list, teaching suggestions, and pre- and posttests with answers) and a student component (competencies, glossary, materials list, activities, and pre- and posttests). The resource section contains a 13-page list of curriculum guides, textbooks, and references; lists of periodicals, publishers, media sources, resource centers, suppliers, and associations; and sample forms. (CML)