This is the story of how an enterprising high school student came to my lab one afternoon, asking if there were any way that he could gain "hands-on" lab experience by working with me. While I had some doubts about allowing him to work in an area with an expensive 150-mW focused laser beam, I eventually said yes. I was well aware that a…

Systems thinking is highly desirable for re-imagining chemistry education, which will help in the development of an integrated and sustainable approach that takes into account the interdependence of a system under study with other components of the ecosystem rather than practicing a fragmented approach. Thus, to develop a systems' perspective into…

We discuss the use of a simple piece of equipment made of a 50 mL syringe attached to a 2 mL graduated pipet to demonstrate Boyle's law and Charles's law. A plot of the hydrostatic pressure against the reciprocal of the volume of the gas read from the equipment is linear as discussed in the paper and gives the atmospheric pressure at the…

This lab experiment uses [superscript 31]P NMR spectroscopy of biomolecules to determine pK[subscript a] values and the binding energies of metal/biomolecule complexes. Solutions of adenosine nucleotides are prepared, and a series of [superscript 31]P NMR spectra are collected as a function of pH and in the absence and presence of magnesium or…

This laboratory experiment utilizes an exploration of the storage stability of beer to introduce basic aspects of electron-paramagnetic-resonance (EPR) spectroscopy. Radicals formed upon aerobic forced-aging of beer samples are established by using a spin-trap. The students are introduced to basic principles of EPR spectroscopy and food and…

This two-part laboratory experiment is concerned with investigating key aspects of the Suzuki-- Miyaura cross-coupling reaction. The first part of this experiment utilizes high-throughput experimentation techniques to reinforce, explore, and extend fundamental concepts that are presented in the classroom. In contrast, the second part employs…

For a variety of reasons, understanding oxidation-reduction (redox) reactions can be challenging for introductory chemistry students. To provide an experiential foundation for students to learn redox concepts, we developed a laboratory experiment that frames redox reactions as a simulated murder mystery. In this experiment, permanganate, which…

During the COVID-19 pandemic, an at-home enzyme assay was developed for a biochemistry laboratory course at Arizona State University. The experiment was designed to use items that could be easily obtained and safe to use. The experiment focused on the analysis of salivary amylase using starch from food as a substrate, black tea as an inhibitor,…

Contribution: This article proposes a low-cost and mobile device-based learning support system for the stepper motor, which provides Web-based remote laboratory. This system allows young engineers to learn about rotational principles, control methods, and programming in stepper motors. Background: Familiarity with electrical machinery, such as…

Solid lipid nanoparticles (SLNs) are exciting nanoparticles used for transporting therapeutic drugs into an organism. In this laboratory work, a simple experiment is performed to introduce master's students into the field of nanotechnology, here applied to health including the applications in the healthcare/pharmaceutical and cosmetic industry.…

A comprehensive undergraduate experiment about extraction, separation, and identification of essential oils (EOs) from a natural plant is described. "Acori tatarinowii" Rhizoma (ATR) was used as the raw plant material. Two devices (Soxhlet and Clevenger) with different extraction principles were employed for EO extraction from ATR,…

The effects of kinetic vs thermodynamic control on "endo"/"exo" stereoisomer ratios can be observed in a simple Diels-Alder reaction between "N"-phenylmaleimide and furan. The use of microwave-promoted synthesis affords the cycloadducts in yields ranging from 65-100%, employing reaction times of 1-10 min at…

We created a 2-week, dual-module summer course introducing high school students to environmental toxicology by teaching them quantitative polymerase chain reaction (qPCR) as a way to quantify gene expression of chemical defense proteins in response to exposure to environmental pollutants. During the course, students are guided through the various…

Students often enter chemistry laboratory courses with a well-documented disconnect between their experiences outside the classroom and the procedures, concepts, and techniques that occur in our courses. Strong base, weak acid titration experiments are present in general chemistry laboratories but also relate to foods our students are familiar…

Hydrogen is a sustainable and climate-friendly storage for renewable energies and can directly be generated from sunlight, e.g., by photocatalytic water splitting. This article presents the photocatalytic hydrogen evolution using LED irradiation of an aqueous ZnS particle dispersion with Na[subscript 2]S and Na[subscript 2]SO[subscript 3] as…