The synthesis of a [2]rotaxane through three- or five-component coupling reactions has been adapted to an organic chemistry experiment for upper-division students. The experimental procedure addresses the search for the most favorable reaction conditions for the synthesis of the interlocked compound, which is obtained in a yield of up to 71%.…

A survey of Oregon State University Department of Chemistry personnel revealed that few of the faculty and graduate student respondents (only 6.7% and 8.3%, respectively) reported knowing the location of the automated external defibrillator (AED) nearest their workspace. Furthermore, a minority of both faculty and graduate student respondents…

This paper uses the questionnaire to evaluate the current status of laboratory safety perceptions, willingness, and efforts of first-year undergraduates at the School of Chemistry and Chemical Engineering, Tianjin University of Technology. The survey includes a sample size of 360 undergraduates covering four chemistry-related majors. The…

The Joint Safety Team (JST) was conceived in 2012 by the Departments of Chemical Engineering and Materials Science and Chemistry at the University of Minnesota and the Dow Chemical Company as a model student-led safety organization. The JST initiative was aimed at improving academic safety through four core areas: compliance, awareness, resources,…

In this article, a proven safety concept with documented success is presented. The concept aligns with best safety practices and the international engineering educational framework termed "The CDIO Initiative," and it has resulted in a strong safety culture among students and staff. This concept has been developed for undergraduate…

The Americans with Disabilities Act allows a student with a disability to bring a service dog into any facility where the public is allowed, including academic teaching and research laboratories. However, the presence of the service dog does have an impact on the safety of the student, the service dog, and others in the laboratory. This article…

Developing strong safety cultures in academic institutions requires that students at all levels be educated by faculty in chemical safety. Yet chemical safety education is missing from the chemistry curriculum. This article considers a report of numerous injuries from incidents from using flammable chemicals in demonstrations as evidence that…

Cola beverages are widely consumed and popular among students; they can be used as safe reagents to replace toxic chemical dyes. In this study, a safe and improved experiment is described, which successfully demonstrates Beer's law and adsorption process using activated carbon as the adsorbent and cola as the adsorbate. The results of this study…

A relatively large number of organic and inorganic chemistry reagents are air- or moisture-sensitive, and undergraduate students should be trained in their use. When handling such reagents, it is important to select the correct syringe and to use that syringe correctly. We have found that the best syringe for use in an undergraduate setting is a…

To prove that oxygen is irreversibly consumed in the blue bottle reaction, a manometer or a plastic bottle was used to show a permanent reduction in the gas pressure in a reaction vessel. This demonstration may be misleading because the change in gas pressure can be attributed to a number of other factors such as temperature change and involvement…

Chemometric techniques such as partial least-squares (PLS) regression have been applied with huge success to a wide array of chemical problems including multicomponent analysis of analytes in complex mixtures. Despite this, there are few examples of laboratory pedagogical exercises that involve students in the acquisition of chemical data from…

While lab accidents that involved personal injuries or significant property damage are required to be reported by law, many minor lab incidents or near misses are less frequently reported, especially in an academic research environment. However, public awareness of these stories and incidents create valuable learning opportunities and can prevent…

The chemistry of metal-organic frameworks (MOFs) has the potential to introduce high school and undergraduate students to the fundamental chemical principles of structure and bonding, enhance the development of skills in synthesis and crystal growth, and promote hands-on experience with gas capture and host-guest chemistry of emerging materials…

A method to synthesize biaryls through the Suzuki-Miyaura cross-coupling reaction using a recyclable fluorous precatalyst is described. This laboratory experiment, which demonstrates the safety benefits of green chemistry, is integrated into an upper-division course. Besides simply using the catalyst for a reaction, students can reuse the catalyst…

Laboratory work in chemistry has been extensively researched in the last decade but the gap between research and practice is still broad. This "Perspective" shares 10 guiding principles relating to university laboratory education, drawing on research over the last decade. Written with an audience of practitioners in mind, the…