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ERIC Number: EJ1458706
Record Type: Journal
Publication Date: 2024-Apr
Pages: 8
Abstractor: As Provided
ISBN: N/A
ISSN: ISSN-0021-9584
EISSN: EISSN-1938-1328
An Improved Potentiostat/Galvanostat for Undergraduate-Designed Electrochemical Laboratories
Joseph S. Elias
Journal of Chemical Education, v101 n4 p1703-1710 2024
We report the design of a low-cost electrochemical workstation and open-source graphical user interface capable of performing a variety of electrochemical methods in an undergraduate teaching laboratory. The instrument--based on the popular Arduino microcontroller board--can be constructed from common components for $40 USD. The modular design of the instrument enables instructors to employ it to fit the needs of their curricula and allows for the acquisition of potentiostatic and galvanostatic data. The incorporation of positive-feedback ohmic drop compensation into the hardware, coupled with the judicious use of signal-averaging within the user-friendly LabVIEW standalone program, allow us to acquire meaningful quantitative electrochemical data (e.g., Tafel slopes) comparable to much more expensive research-grade potentiostats. The companion program is available free of charge online and vastly improves the scope of electrochemical methods available to undergraduate laboratories. We demonstrate the versatility of this potentiostat/galvanostat by employing it in General Chemistry and Inorganic Chemistry courses in modules that touch on sustainability, renewable energy, and electrocatalysis. We hope these improvements will enable instructors to incorporate electroanalytical techniques into their undergraduate curricula and empower the next generation of scientists to take full advantage of these methods in their research.
Division of Chemical Education, Inc. and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
Publication Type: Journal Articles; Reports - Descriptive
Education Level: Higher Education; Postsecondary Education
Audience: N/A
Language: English
Sponsor: N/A
Authoring Institution: N/A
Grant or Contract Numbers: N/A