A new teaching resource comprised of raw X-ray diffraction data sets from crystallography experiments has been compiled. The aim of this resource is to provide a tool with which to plug the teaching gap between crystals and chemical structures present at various levels of education, as well as providing examples for early stage researchers and…

Owing to the critical role of stereochemistry in biotechnology, medicine, and industry, it must be well represented in undergraduate lab curricula. To achieve these stereochemical laboratory requirements without sacrificing existing lab techniques, we modified two standard laboratory experiments to include chiral GC analysis as follows. (1) The…

Using polymerizable cholesteric liquid crystal (CLC) paints, we prepare circularly polarized freestanding films that enable students to acquire a basic understanding of circular polarization and molecular chirality. The polymerized helical structures of CLC films can exhibit brilliant structural colors by selective reflection of visible light…

This exercise encompassed the construction and use of a microcontroller-based laser refractometer. The instrument, which does not require a high skill level to build, primarily consisted of a line laser, optical sensor, several 3-D printed parts and printed circuit boards, and a microcontroller development board. Construction and testing of the…

The methodology and mathematical treatment of several classic multivariate methods for the analysis of spectroscopic data is demonstrated in a straightforward way that can be used as a basis for teaching an undergraduate introductory course on chemometric analysis. The multivariate techniques of classical least-squares (CLS), principal component…

In the vicinity of a critical point, the impact of a substance's chemical identity is superseded by universal critical behavior for a number of physical properties, such as visible light scattering. In this classroom demonstration, students observe a single-phase critical mixture of partially miscible isobutyric acid + water (IAW) as the…

Nanoparticles are an increasingly important tool in chemistry research, but currently there are few opportunities for chemistry students to work with nanoparticles in undergraduate analytical courses. In this exercise, designed for an analytical or instrumental analysis lab course, students have the opportunity to work with solutions of silver…

Nowadays, technologies involving nanoparticles, colloids, sensors, and artificial intelligence are widespread in society, media, and industry. It is thus mandatory to integrate them into the curricula of students enrolled in chemistry and materials science. To this purpose, we designed a simple assay for the detection of glutathione (GSH) using…

Optical polarization phenomena are omnipresent in physics, chemistry, biology, and technology. Studying optical polarization is best done through an interdisciplinary approach that combines biology and technology, which usually makes things more interesting to students. Seeing Haidinger's brush for the first time can be an exciting discovery for…

In this communication, a remote experimental activity in chemical kinetics is described, taking into account the quantification based on the optical sensor of a smartphone. The objective pursued herein is to equip students with the appropriate tools and strategies required to empirically determine the parameters of the rate law including reaction…

Computer vision (CV) is a subfield of artificial intelligence (AI) that trains computers to understand our visual world based on digital images. There are many successful applications of CV including face and hand gesture detection, weather recording, smart farming, and self-driving cars. Recent advances in computer vision with machine learning…

A low-cost time-resolved emission spectrometer optimized for ruby emission is presented. The use of a Class II diode laser module as the excitation source reduces costs and hazards. The design presented here can facilitate the inclusion of time-resolved emission spectroscopy with laser excitation sources in the undergraduate laboratory curriculum.…

Pulsed field gradient nuclear magnetic resonance (NMR) is used to estimate the size of quantum dots (QDs) produced in a simple, fast, small-scale synthesis. This upper-division laboratory experiment teaches the basics of QD synthesis and pulsed field gradient NMR, a powerful technique for measuring diffusion coefficients in solution. The diffusion…

A spin coater is widely used for thin film coating in nano/microtechnology. In this paper, a spin coater with inexpensive mechanical and electronic components was fabricated based on an open-source Arduino microcontroller. To measure and control the spin speed of the spin coater, two sensor types including two infrared (IR) light-emitting diodes…

Students in an upper-level physical chemistry course used a polarimeter to measure the molar optical rotation of different optically active amino acids to confirm the Clough, Lutz, and Jirgensons (CLJ) rule. This rule states that an amino acid is in the l-configuration if the molar optical rotation becomes more positive upon the addition of acid…