This manuscript describes a laboratory exercise that allows students to use conductive atomic force microscopy (CAFM) for the analysis of electrodeposited, metallic structures. In addition to nanoscale electrical characterization with CAFM, this laboratory exercise also provides students with an opportunity to explore nanofabrication by…

The essential component of expanding an undergraduate curriculum is the inclusion of lab experiments in nanoscience and nanomaterials, which significantly impact health and the environment through their use in food, cosmetics, agriculture, and medicine. We designed a laboratory experiment based on the atomic force microscopy (AFM) analysis of the…

Artificial intelligence (AI) is receiving a lot of attention in various fields. There is a need for educating students in AI technology. In this context, we have created a new type of carbon dioxide fountain by integrating AI with the well-established Arduino-carbon dioxide fountain experiment. This experiment consists of an Arduino…

A handheld refractometer (HHR) is a versatile instrument in the chemistry lab or in the workplace. It is also inexpensive enough (<$25 U.S.) that all students in a chemistry lab can have one or students completing laboratories remotely can purchase one. We report four applications of two different HHRs: one HHR for which the scale reads…

We present a modernization of the undergraduate physical chemistry laboratory experiment for determining the speed of sound in various gases from resonant frequencies in a spherical resonator. The resonator (schematic IR = 7.5 cm) is constructed by 3D printing with eco-friendly poly(lactic acid), a commercially viable alternative to traditional…

We propose an apparatus that emulates the experiment used by Geiger and Marsden in 1913 to investigate alpha particles (Rutherford) scattering. Using a widely available fused deposition modelling 3D-printer, we built a compartmented and easily assembled educational instrument. The whole apparatus is composed of a 3D-printed chamber and an…

In this laboratory experiment, students explore the aquatic photochemical fate of ranitidine and cimetidine, two common pharmaceutical pollutants found in wastewater. It provides an engaging environmental context for students to develop knowledge of reaction kinetics and photochemistry as well as skill in using analytical instrumentation. This…

During the SARS-2-COVID pandemic our institution sought to continue the teaching and learning of experimental laboratories by designing, assembling, and delivering a microscale chemistry kit to the students' homes. Thanks to this approach students were able to perform [approximately]25 experiments during each one of the Fall 2020 and Spring 2021…

A fluorometer is a device that measures the spectroscopic properties of fluorescent materials, and fluorometry is used widely in chemistry research settings to characterize fluorescent samples. One of the obstacles faced by undergraduate programs looking to implement fluorometer-based experiments into their laboratory curriculum is the high cost…

In this article we describe the construction of a low-cost electronic device to adapt the widespread traditional approach of Analytical Chemistry teaching into laboratory experimentation based on the guided research model. To this aim we construct a portable electronic instrument based on the Arduino microcontroller and use it to develop various…

We describe an experiment in which students use research-grade instrumentation to collect gas adsorption data in triplicate in a single 3 h laboratory period. The experiment reinforces the thermodynamic concepts taught in upper level physical chemistry courses and hands-on experience with instrumentation used in research laboratories. The speed of…

Thin-layer chromatography, which involves the movement of dyes along a silica-coated plate, is used to observe the progress of chemical reactions and to separate mixtures. We took advantage of this phenomenon to devise a method for generating patterns in the shape of numbers with dots (dot matrix). We prepared the azo dyes necessary for generating…

Experimental electrochemistry offers unique opportunities for interactive instruction at all levels of education; however, widespread adoption in curricula is hindered by high costs associated with electrochemical instrumentation. Thus, the development of affordable instruments represents an essential step toward making electrochemistry accessible…

There currently exists a significant deficiency in the nuclear chemistry workforce within the United States, despite its importance in areas of medicine, national security, and energy. Poor coverage of this topic across many chemistry departments at the undergraduate level likely contributes to this shortage. Increasing interest and hands-on…

The ability to visualize chemical processes can be an asset in a teaching laboratory. Despite the advances in laboratory technology, apparatuses used in the teaching of simple thermodynamics concepts, such as exothermic/endothermic reactions, historically remain unchanged and can benefit from a fresh perspective. The recent incorporation of…