Chemists have always designed and deployed cross-disciplinary approaches that interface chemistry with other disciplines to proffer solutions to many human problems. We designed a laboratory experiment that implements chemistry concepts in a biological model to prime undergraduate students to appreciate interdisciplinarity as an approach to…

Millions of people do not have access to clean drinking water; thus, cost-efficient water treatment systems are vital. Chemists, environmentalists, technicians, and engineers will be the professionals making breakthroughs in this industry. This laboratory experiment aims to introduce undergraduate students to the removal of pollutants from water…

We present a modernization of the undergraduate physical chemistry laboratory experiment for determining the speed of sound in various gases from resonant frequencies in a spherical resonator. The resonator (schematic IR = 7.5 cm) is constructed by 3D printing with eco-friendly poly(lactic acid), a commercially viable alternative to traditional…

In this laboratory experiment, students explore the aquatic photochemical fate of ranitidine and cimetidine, two common pharmaceutical pollutants found in wastewater. It provides an engaging environmental context for students to develop knowledge of reaction kinetics and photochemistry as well as skill in using analytical instrumentation. This…

The use of mass spectrometry (MS) is becoming widespread and rather routine in all levels of industry, government, and academia. Coupled with chromatographic methods, this powerful instrumental technique can be used to elucidate the composition of a complex sample and definitively identify constituents while offering the benefits of high-precision…

Given the severe pollution caused by traditional plastics, biodegradable plastic products (BPPs) have received great attention and are appearing in people's lives in the form of packaging bags, tableware, etc. Whether a wide variety of BPPs can truly degrade depends on the environment. Aerobic composting is the arbitration method to evaluate the…

For the past century, humans have been increasingly dependent on plastics, but have not developed adequate disposal practices. In this lab, students are asked whether burning plastic for energy seems like a reasonable disposal technique. To answer the chemical aspects of this question, students use bomb calorimetry to quantify the combustion…

Students determine the iron mass in dietary supplements using four colorimetric assays. These colorimetric assays were selective for Fe[superscript 3+]. It was complexed by thiocyanide, salicylate, gallic acid, and Fe(CN)[subscript 6][superscript 4-], forming blood-red, red, violet, and blue complexes, respectively. The [lambda][subscript max] of…

A set of inexpensive and pedagogically rich experiments focusing on S[subscript N]1, E1, and E2 reactions have been updated to include modern computational and spectroscopic analyses. The S[subscript N]1 experiment involves treatment of "tert"-amyl alcohol with hydrochloric acid to generate the corresponding alkyl chloride, which is used…

This laboratory experiment introduces students to an important reaction in biomass valorization and allows them to gain a practical understanding of green chemistry. Acid-catalyzed dehydration reactions of fructose to 5-hydroxymethylfurfural and thus humins were performed both with and without aqueous solvent, along with two different catalysts…

To deliver state-of-the-art battery knowledge to undergraduates, we designed a feasible experiment to prepare flexible packaging batteries, aiming to reproduce industrial flexible packaging batteries in general chemistry laboratories. In our procedure, the materials involved are inexpensive, safe, and easy to use. No organic solvents or toxic…

The concept of equilibrium vapor pressure plays a key role in the general chemistry curriculum; it is among the first and most easily demonstrated examples of equilibrium and frequently caps off the first semester of general chemistry where it illustrates the properties of liquids and intermolecular forces. We report here simple modifications of…

Water electrolysis, a well-known and simple experiment, confirms that a water molecule comprises hydrogen and oxygen atoms. In this experiment, hydroxide or hydrogen ions generated from each electrode were identified using an indicator based on the assumption that electrodes, electrolytes, and indicators do not participate in the water…

Keto-enol tautomerism is a special example of structural isomerism. In this experiment, 6-chlorofulvene is predominantly yielded during the chlorination reaction of 6'-hydroxyfulvene with POCl[subscript 3] in the presence of DMF. The high regioselectivity of this reaction is dominated by intramolecular hydrogen-bonding and steric hindrance,…

The study of gels and their properties is a compelling topic both technologically and scientifically, and should therefore be emphasized in chemistry and material science syllabuses. In the present laboratory experiment, we propose two experiences, aimed at introducing gelation and gel transport properties using silica gels made from sodium…