This research developed learning activities for students to explore and connect the concepts of acid-base titration, equivalence points, pK[subscript a], and molar absorption coefficients. Polyphenolic compounds consisting of p-coumaric acid (CMA), caffeic acid (CFA), and 3,4,5-trihydroxycinnamic acid (3,4,5-THCA) were selected as study models.…

A straightforward procedure for the synthesis of (Ph[subscript 3]P)[subscript 3]CuCF[subscript 3], a robust, air-stable trifluoromethylating agent, is reported herein. This preparation can be completed in a single 3 h laboratory session and typically provides ample yields (~79--86%) and high purity (>90%). The target complex is characterized by…

TNT is both toxic and explosive, and therefore, the detection of TNT represents an environmental concern and a security concern. Dogs are often used for detection, but other methods are needed. This laboratory investigates a ruthenium bipyridine ([Ru(bpy)[subscript 3]][superscript 2+]) luminescence-based trinitrotoluene (TNT) sensor. Students will…

Nanoparticle synthesis is an important area of nanotechnology and has been performed by undergraduate students from various universities across the globe. Due to the availability of massive data on the synthesis of a wide variety of metallic nanoparticles, including silver, gold, selenium, zinc, copper, iron, palladium, platinum, titanium, etc.,…

In the face of an increasingly severe global climate change situation, carbon neutrality initiatives have been included in the development action plans of many countries around the world. The carbon neutrality vision will also accelerate the revolution in the energy systems of countries around the world, injecting new vitality into the upgrading…

As a cross-cutting and comprehensive subject, medicinal chemistry involves the knowledge of chemical, biological, medical, and pharmaceutical sciences. A comprehensive medicinal chemistry experience for undergraduates is expected to train various experimental skills and enhance their scientific research ability. Herein, a series of laboratory and…

Level 3 characteristics are increasingly important for fingerprint identification, particularly when the fingerprints are problematic and lack level 2 details. In practice, no reliable visualization methods for level 3 features are transferred into a course for the general public, forensic students, or investigators. Our group has reported the…

The COVID pandemic forced teachers to be imaginative, especially with purely practical subjects such as laboratory chemistry. In the Universidad Nacional Autónoma de México, the first-semester chemistry laboratory of the Biology course was taught with a chemistry set to be used at home. The use of the kit was evaluated from the perspective of…

Computational chemistry instructional activities are often based around students running chemical simulations via a graphical user interface (GUI). GUI-based activities offer many advantages, as they enable students to run chemical simulations with a few mouse clicks. Although these activities are excellent for introducing students to the…

In 1996, the Chemistry Department at Norwich University converted its two-semester General Chemistry course from a traditional lecture to a Process Oriented Guided Inquiry Learning (POGIL) classroom. The change to POGIL teaching in Norwich General Chemistry classes was brought about by a steady decline in student performance, as demonstrated by…

As teaching laboratories stand empty in light of COVID-19, we extended the practical experience from the laboratory to the safety of the students' homes. We developed a simple, robust, and versatile at-home experiment that teaches solution preparation, calibration curves, real-life sample preparation, and data analysis to second-year analytical…

The identification of coloring substances is a relevant task in the field of conservation and restoration, but it can be challenging as in real samples the target analytes are inserted in a very complex matrix made of binders and additives. Understanding this concept is fundamental for upper-division undergraduate students interested in…

Curriculum-based undergraduate research experiences (CUREs) have been shown to increase student retention in STEM fields and are starting to become more widely adopted in chemistry curricula. Here we describe a 10-week CURE that is suitable for a second-semester organic chemistry laboratory course. Students synthesize small molecules and use…

The laboratory experiment regarding esterification of ethylene glycol with acetic acid to ethylene glycol diacetate using resin catalysts in a continuous flow was designed to carry out the reaction in a flow through an inquiry-guided approach. Incorporating the burgeoning field of continuous flow chemistry into the educational infrastructure, the…

An NMR tube cleaner that is quickly and easily constructed from everyday laboratory equipment is described. This cost-effective option removes the need to purchase a fragile, more expensive model. The small footprint of the device lends itself to being given a permanent place in the laboratory, but it is also simple enough to disassemble and…