Learning in chemistry laboratories has long been challenging due to the complex nature of the learning environment and tasks that students engage with. Therefore, it is important to develop useful tools for prelab and follow-up activities besides the hands-on lab time for better management of the learners' cognitive load. In this paper, we…

A laboratory experiment was designed to provide students with an introduction to byproduct valorization by producing an analogue of biodiesel (fatty acid ethyl esters, FAEE) via lipid extraction and subsequent transesterification from spent coffee grounds (SCG). Valorization is the process of upgrading underutilized or discarded wastes or…

Potash, an essential raw material of the 18th century, used to be produced from the ashes of plants. Known since antiquity, it was in 1807 that Humphry Davy put an end to the decades-long controversy about its nature as a compound. The technology behind potash production was implemented in Brazil by the Portuguese naturalist Frei Velloso. The…

This laboratory experiment consists of the synthesis of two series of alkaline-earth titanates (calcium-strontium and strontium-barium)to corroborate Vegard's law by obtaining their X-ray diffraction patterns and plotting the lattice parameter versus mole fraction of both cations. This experiment allows students to understand the key concepts in…

A [beta]-lactam, the core structure unit of clinically important antibiotics such as penicillin and cephalosporin, is one of the most commonly encountered four-membered heterocycles in organic chemistry and is widely used in medicine and biochemistry. The Kinugasa reaction, a copper­(I)-catalyzed cycloaddition of a terminal alkyne with a nitrone,…

An experimental design by combining hydrogel and ethylenediaminetetraacetic acid disodium salt (EDTA) for visually displaying chemical complexation reactions is developed. The Na[superscript +] ions on the [alpha]-l-guluronic acid (G) unit of the sodium alginate molecule undergo an ion exchange with a divalent cation, so that the G units are…

We describe an experiment in which students use research-grade instrumentation to collect gas adsorption data in triplicate in a single 3 h laboratory period. The experiment reinforces the thermodynamic concepts taught in upper level physical chemistry courses and hands-on experience with instrumentation used in research laboratories. The speed of…

This article describes an enrichment and extension of a published applied chemistry experiment involving the use of distilled fragrant compounds of natural plants to prepare facial toner. The original protocol failed to consider quality evaluation of the self-prepared facial toner. Herein, an additional experimental section is included for…

E-learning is not a new concept to the American University of Nigeria (AUN); however, it has always been applied to the lectures but not in the laboratories for the chemistry courses before and during the first phase of the COVID-19 lockdown. The sudden disruption of learning caused by the forced lockdown issued by the government authority in an…

This work describes the design and testing of a low-cost light-emitting diode (LED)-based nephelometer for turbidity analysis. It also describes the use of this nephelometer for context-based learning (CBL) experiments designed for teaching laboratories. The LED nephelometer is simple, low-cost, and robust, providing similar results as a…

Successful demonstration of lipid assembly chemistry to a general audience can be challenging on both physical (nanoscopic dimensions of lipid assemblies) and intellectual (complex, interconnected concepts) accounts. Quite often, an instructor has to leave key concepts out of what is being offered due to time constraints, which unfortunately…

Virtual chemistry laboratory modules were investigated as a potential learning resource that complements traditional in-person experiments. In collaboration with a high school instructor, we designed two interactive modules, "Rates of Reaction" and "Models of Organic Molecules," which became part of a previously reported online…

"Copper to Silver to Gold: The Alchemist's Dream" is an experimental demonstration performed in many schools that involves Zn plating on a Cu coupon to induce brass plating. In this study, a novel method to achieve uniform plating is proposed using a 2.0mol/L ZnCl[subscript 2] aqueous solution, sodium dodecyl sulfate, and Al foil. This…

The principles of process-oriented guided inquiry learning (POGIL) are applied to the analysis of the emission spectrum of atomic hydrogen. Over the course of three learning cycles, students construct the hydrogen atom's energy level diagram and assign quantum numbers using their measurements of the Balmer series plus additional information on the…

Green chemistry is finding its place as one of the most essential study topics in the curriculum of future chemists and chemical engineers. Experiments that meet green chemistry principles contribute to make the laboratory a safer working place, generate less waste, and allow students to increase their knowledge in new environmentally friendly…