Offers challenging work at a higher level of technique than most students meet in elementary laboratory work. Uses a combined weight and volumetric sequence not shown in textbooks. Notes modern rapid balances help lower evaporation loss during weighings. Discusses the balance, weights, and buoyancy considerations. (MVL)

Discusses the need to encourage increasing numbers of persons to enter analytical chemistry, educate them thoroughly in basic chemical science, and expose them to the most modern methods and instrumentation. Examines some problems and several university's efforts to overcome them. (MVL)

Discusses three areas of catalysis: homegeneous, heterogeneous, and enzymatic. Explains fundamentals and economic impact of catalysis. Lists and discusses common industrial catalysts. Provides a list of 107 references. (MVL)

Describes a crystallography experiment using both diffraction-angle and diffraction-intensity information to determine the lattice constant and a lattice independent molecular parameter, while still employing standard X-ray powder diffraction techniques. Details the method, experimental details, and analysis for this activity. (CW)

Presented is a classification of polymers according to physical condition. Considered are molecular structure and arrangements. Described are demonstrations using polarized light and the mechanical properties of polymers. (CW)

All analytical techniques depend on the use of calibration chemicals to relate analyte concentration to instrumental parameters. Discusses the preparation of standard solutions and provides a critical evaluation of available materials. Lists elements by group and discusses the purity and uses of each. (MVL)

Discusses two computer problem solving programs: rule-based expert systems and decision analysis expert systems. Explores the application of expert systems to automated chemical analyses. Presents six factors to consider before using expert systems. (MVL)

States that quantitative modelling allows teachers to concentrate more on qualitative understanding. Suggests the main benefits as (1) repetitive calculations are reduced allowing greater attention to be focused on underlying models; (2) more "what if" models can be tested; and (3) a wider variety of data can be used to test models. (MVL)

Describes a laboratory experiment to teach the principles of air sampling, gamma ray spectroscopy, nuclear decay, and radioactive equilibrium. Analyzes radon by carbon adsorption and gamma ray counting. Provides methodology and rate of decay equations. (MVL)

Examines two computer interfaced lab experiments: 1) discusses the automation of a Perkin Elmer 337 infrared spectrophotometer noting the mechanical and electronic changes needed; 2) uses the Gouy method and Lotus Measure software to automate magnetic susceptibility determinations. Methodology is described. (MVL)

Clarifies the roles of a practicing analytical chemist in industry: quality control, methods and technique development, troubleshooting, research, and chemical analysis. Lists criteria for success in industry. (ML)

Identifies a common laboratory problem that causes instrumentation malfunction. Provides numerous experiences of researchers whose results have been affected by humidity fluctuations, magnetic field fluctuations, trucks driving by, and other factors. (ML)

Considers three common cases of localized corrosion of metals: pitting, crevice, and stress corrosion. Provides experimental methods for studying all three methods. Includes a discussion of expected results. (ML)

Describes an experimental procedure for determining trihalomethanes (THMs) in liquids by gas chromatography. Provides recommendations for reactants and supplies to obtain acceptable results. Discusses the analysis of water from various sources: pools, lakes, and drinking water; compares these to three cola drinks. (ML)

Project Chemlab was designed to prepare an "Annotated List of Laboratory Experiments in Chemistry from the Journal of Chemical Education (1957-1979)" and to develop a computer file and program to search for specific types of experiments. Provided in this document are listings (photoreduced copies of printouts) of over 1500 entries…