A material commonly known as Flubber, with properties that are excellent for teaching about glaciers, has been widely used in geosciences education. Yet, the original recipe contains borax, which has health risks that should be avoided. A new recipe is shared containing low-cost, readily available ingredients that produces a reformulated Flubber…

Polychlorinated biphenyls (PCBs) are a family of synthetic chemicals consisting of carbon, hydrogen, and chlorine atoms. PCBs have been produced commercially since 1929 in hundreds of industrial applications. Their continued production in the United States was phased out in the late 1970s, and strict disposal guidelines were regulated as adverse…

Arsenic is a toxic element to which humans are primarily exposed through food and water; it occurs as a result of human activities and naturally from the earth's crust. An experiment was developed for a senior level analytical laboratory utilizing an Inductively Coupled Plasma-Mass Spectrometer (ICP-MS) for the analysis of arsenic in household…

We present a collection of hands-on experiments that collectively teach precollege students fundamental concepts of polymer synthesis and characterization. These interactive experiments are performed annually as part of an all-day outreach event for high school students that can inform the development of ongoing polymer education efforts in a…

This project involved developing a method to remediate large quantities of aqueous waste from a general chemistry laboratory experiment. Aqueous Ni(II) waste from a general chemistry laboratory experiment was converted into solid nickel hydroxide hydrate with a substantial decrease in waste volume. The remediation method was developed for a…

Investigations that integrate concepts from geological sciences with biology and chemistry are rare. The authors present an investigation that introduces high school students to microbe-mineral interactions by tying together anaerobic respiration, reduction reactions, metal ion solubility, and groundwater pollution. During the investigation,…

A sequence of exercises for the isolation and characterization of invertase (E.C. 3.1.2.26) from baker's yeast obtained from a local grocery store is outlined. Because the enzyme is colorless, the use of colored markers and the sequence of purification steps are designed to "visualize" the process by which a colorless protein is selectively…

Virstatin, an "N"-butanoic acid substituted naphthalimide, inhibits the ability of "Vibrio cholerae" to cause disease. A three-week experiment involving synthesis, purification, and spectral characterization of this compound is described. This experiment is appropriate for organic chemistry. It has been performed with three lab sections of about…

A microscale laboratory experiment to investigate the formation and utility of microemulsions is described. Microemulsions are technologically important fluids that can reduce the use of toxic organic solvents. In the experiment, students prepare a microemulsion and compare the solubility of sudan III dye in the microemulsion and in dodecane. They…

In this experiment, organic chemistry students perform reactions between three naphthyl acetate derivatives and the diazonium salt Fast-Red TR, under basic conditions. The three naphthyl acetate derivatives used in this study are 2-naphthyl acetate (1a), 6-bromo-2-naphthyl acetate (1b) and 1,6-dibromo-2-naphthyl acetate (1c). The two-step, one-pot…

The guide presents information about ordering, using, storing, and maintaining chemicals in the high school laboratory. The guide also provides information about chemical waste, safety and emergency equipment, assessing chemical hazards, common safety symbols and signs, and fundamental resources relating to chemical safety, such as Material…

Presents a scenario related to the disposal of potentially dangerous ether. Several suggestions for dealing with peroxide-forming compounds are included. (JN)

Procedures for recovering silver and cobalt from laboratory wastes (including those resulting from student experiments) are presented. The procedures are generally applicable since only common, inexpensive laboratory reagents are needed. (JN)

Presents a model, ChemSafe, that was developed to address and solve the allied problems of chemical purchase, storage, use, and disposal in schools. (ZWH)

Chemical demonstrations can and do enhance an otherwise potentially dull subjects--the properties of hazardous materials. This book contains the recipes for presenting several chemical demonstrations. Demonstrations are designed to be relatively easy to perform and present minimal hazards if done properly. The book contains an introduction, safety…